Skip Navigation

University of Nebraska–Lincoln

Central Facility for Electron Microscopy

Nebraska Center for Materials and Nanoscience

VG HB-5 Scanning Transmission Electron Microscope

 

The VG HB-5 Scanning Transmission Electron Microscope (STEM) is a high resolution combination of a SEM and TEM, giving it the abilities of both. Chief among the uses of such an instrument are its excellent compositional capabilities; able to detect a single heavy atom in a spot a few nanometers wide.

Some facts about the STEM:

  • Accelerating voltage: 100kV
  • Room Temperature Field Emission Electron Source (high brightness)
  • Vacuum system capable of 1 x 10-12 Torr
  • Sample tilting: 45°
  • Heated (500°C) and cooled (liquid nitrogen) stages
  • Capable of reactive gas introduction at controlled rates
  • Equipped with Secondary and Backscattered detectors for SEM type work
  • Capable of Bright Field, Annular Dark Field, SAED and CBED imaging
  • Equipped with EDS capable of detecting Boron and forming X-ray maps of composition; composition to within 0.1 wt%
  • Areas as small as 1 nm in diameter can be accurately characterized with EDS, diffraction and imaging
  • Maximum sample size: 5 mm diameter, 2 mm thickness disk
  • Digital imaging system capable of image capture and storage in electronic form (TIFF)
  • High quality, medium cost Polaroid type 55 film output, yielding both a negative and positive image

VG HB-5 STEM

 

 

 

 

 

 

 

 

 

 

 

 

STEM sample results:

 

carbon

A sample output of the direct writing of iron lines on carbon. The magnification is 50,000 times.